Search results for " X-ray photoelectron spectroscopy"
showing 5 items of 5 documents
Oxidation State and Local Structure of Chromium Ions in LaOCl
2021
This research is funded by the Latvian Council of Science, project “Novel transparent nanocomposite oxyfluoride materials for optical applications”, project No. LZP-2018/1-0335. Institute of Solid State Physics, University of Latvia as the Center of Excellence has received funding from the European Union’s Horizon 2020 Framework Programme H2020-WIDESPREAD-01-2016-2017- TeamingPhase2 under grant agreement No. 739508, project CAMART2.
Carbon nanotubes thin filters for x-ray detectors in space
2022
In this paper, we present the first results from an investigation performed on nanometric thin pellicles based on carbon nanotubes (CNT) of potential interest for manufacturing large area optical blocking filters to protect soft X-ray detectors in astrophysics space missions. In order to evaluate the effective capability of such materials to block UV/VIS/IR radiation, while being highly transparent in the soft X-rays and strong enough to withstand the severe launch stresses, we have performed a suite of characterization measurements. These include: UV/VIS/IR and X-ray absorption spectroscopy, X-ray Photoelectron Spectroscopy and Scanning Electron Microscopy on bare and Al coated small self-…
Smooth crack-free targets for nuclear applications produced by molecular plating
2013
The production process of smooth and crack-free targets by means of constant current electrolysis in organic media, commonly known as molecular plating, was optimized. Using a Nd salt, i.e., [Nd(NO3)(3)center dot 6H(2)O], as model electrolyte several constant current density electrolysis experiments were carried out to investigate the effects of different parameters, namely the plating solvent (isopropanol and isobutanol mixed together, pyridine, and N,N-dimethylformamide), the electrolyte concentration (0.11, 0.22, 0.44 mM), the applied current density (0.17, 0.3, 0.7, and 1.3 mA/cm(2)), and the surface roughness of the deposition substrates (12 and 24 nm). Different environments (air and …
Hard x-ray photoelectron spectroscopy: a snapshot of the state-of-the-art in 2020
2021
Journal of physics / Condensed matter 33(23), 233001 (1-44) (2021). doi:10.1088/1361-648X/abeacd
N-Doped Anatase/Rutile Photocatalysts for the Synthesis of Aromatic Aldehydes Under Ultraviolet and Solar Irradiation
2015
N-doped anatase/rutile photocatalysts were prepared by a sol-gel method, using TiCl4 as TiO2 precursor and urea as N-dopant source. The catalysts required a thermal treatment at temperature higher than 300 degrees C to achieve actual nitrogen doping; this treatment also allowed obtaining crystalline and hydrophobic samples. Moreover, nitrogen doping modified the surface of samples by increasing the anatase to rutile phase ratio and hydrophilicity. The catalysts were characterized by BET specific surface area, XRD, ESEM, TGA, FT-IR, DRS and XPS measurements, with particular attention to the assessment of the N-doping effect. It was found that XPS analysis should be used together with DRS and…